In short: Treat the porous silica as a candidate substrate, not as an adsorbent: functionalise it with your own chemistry, run batch adsorption on a real or synthetic effluent against a reference medium, and only then move to a column. Sensilchem supplies CENSIL 320 as the primary substrate with 310 and 500 as comparison points; the untreated silica is not a validated fluoride adsorbent and no removal performance is claimed.
Run the raw silica through your own surface and pore characterisation so that later changes can be attributed to the functionalisation. Keep a sample of each untreated grade as the baseline.
Apply the same chemistry, ratio, temperature and washing to each grade in the same session. The comparison is between substrates, so the treatment must not be a variable.
Shake a fixed mass of each functionalised substrate with the effluent at the pH the plant actually runs, alongside the reference medium, and measure residual fluoride at set times. Report the reference result in the same table — that is what makes the screening readable.
Industrial effluents carry sulphate, phosphate and bicarbonate that compete for sites. Repeat the batch test on the real effluent, not only on a synthetic fluoride solution.
Pack a small column with the leading functionalised substrate and run breakthrough at a realistic flow. Batch capacity and column performance diverge, and the column is what the plant will see.
Regenerate with the eluent you intend to use and re-run the column. A substrate that performs once and collapses on regeneration is a consumable, not a treatment step.
No claim is made for the untreated material. The porous grades are candidate substrates for a treatment developer's own functionalisation and screening programme.
Surface development and pore volume differ across 310, 320 and 500, and the screening is meant to show which substrate your chemistry works best on.
The material you use now, the formulation or resin, the equipment and the target you need to hit. That is enough for us to say whether we have something worth testing.
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